Yale University

Source: https://cbic.yale.edu/instruments-view/a500b Parent: https://cbic.yale.edu/instruments/experiment-runtime-estimation

A500b Agilent DD2 500 MHz NMR Spectrometer (Manual)

Short Name:

A500b

Instrument Type:

NMR & EPR

Location:

KCL 3

Date of Acquisition:

September 2012

Description:

2 channel system, OneNMR probe with auto-tune-and-match installed.

Best experiments:

Acceptable experiments:

Not available:

Time Required for NMR Experiments on A500b:


Mass	Concentration	Proton	Carbon	gCOSY	gHSQC	gHMBC
0.03 mg	0.1 mM	5 hours	16962 hours	67 h 16 min	820 h 42 min	3113 h 37 min
0.06 mg	0.2 mM	1 h 10 min	424 h 02 min	16 h 50 min	205 h 15 min	779 h 06 min
0.15 mg	0.5 mM	0 h 11 min	678 h 28 min	2 h 45 min	32 h 50 min	124 h 34 min
0.3 mg	1 mM	0 h 03 min	170 h 00 min	0 h 42 min	8 h 20 min	31 h 09 min
0.6 mg	2 mM	< 1 min	4 h 15 min	0 h 11 min	2 h 05 min	7 h 48 min
1.5 mg	5 mM	< 1 min	3 h 11 min	0 h 03 min	0 h 08 min	1 h 40 min
3 mg	10 mM	< 1 min	1 h 42 min	0 h 03 min	0 h 08 min	0 h 17 min
6 mg	20 mM	< 1 min	0 h 25 min	0 h 03 min	0 h 08 min	0 h 17 min
12 mg	40 mM	< 1 min	0 h 06 min	0 h 03 min	0 h 08 min	0 h 17 min
15 mg	50 mM	< 1 min	0 h 04 min	0 h 03 min	0 h 08 min	0 h 17 min
> 30 mg	100+ mM	< 1 min	0 h 04 min	0 h 03 min	0 h 08 min	0 h 17 min

All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube

Instrument Image: